Polymeric iodobismuthates Cat{[BiI4]} with pyridinium-derived cations: structure and properties

Мұқаба

Дәйексөз келтіру

Толық мәтін

Ашық рұқсат Ашық рұқсат
Рұқсат жабық Рұқсат берілді
Рұқсат жабық Рұқсат ақылы немесе тек жазылушылар үшін

Аннотация

Two novel bismuth(III) iodide complexes – (1,3,4-MePy){[BiI4]} (1) и (3-Br-1-MePy){[BiI4]} (2)) – were synthesized by the reaction of iodides of corresponding cations with BiI3 in organic solvents. Crystal structure of the compounds was determined by X-ray diffraction; For both complexes, the thermal stability was studied, and the optical band gap values were experimentally estimated.

Толық мәтін

Рұқсат жабық

Авторлар туралы

I. Shentseva

Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences

Email: usoltsev@niic.nsc.ru
Ресей, Novosibirsk, 630090

A. Usoltsev

Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences

Хат алмасуға жауапты Автор.
Email: usoltsev@niic.nsc.ru
Ресей, Novosibirsk, 630090

N. Korobeynikov

Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences; Novosibirsk State University

Email: usoltsev@niic.nsc.ru
Ресей, Novosibirsk, 630090; Novosibirsk, 630090

I. Korolkov

Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences

Email: usoltsev@niic.nsc.ru
Ресей, Novosibirsk, 630090

M. Sokolov

Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences

Email: usoltsev@niic.nsc.ru
Ресей, Novosibirsk, 630090

S. Adonin

Nikolaev Institute of Inorganic Chemistry, Siberian Branch, Russian Academy of Sciences; Irkutsk Favorsky Institute of Chemistry SB RAS

Email: usoltsev@niic.nsc.ru
Ресей, Novosibirsk, 630090; Irkutsk, 664033

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2. Fig. 1. Crystal packing of compound 1 along the crystallographic axis a.

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3. Fig. 2. Br---I contacts (dashed line) in crystal structure 2. Hydrogen atoms are not shown.

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4. Fig. 3. Stacking interactions in the structures of compounds 1 and 2. For C---Br interactions the distances are signed.

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5. Fig. 4. Powder diffractograms of compounds 1 (a) and 2 (b): black - calculated, red - experimental.

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6. Fig. 5. TG, DTG and DTA curves for compounds 1 (a) and 2 (b).

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7. Fig. 6. Diffuse reflectance spectra of compounds 1 (a) and 2 (b).

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